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Technical Development


ScienceAsia 9 (1983): 175-185 |doi: 10.2306/scienceasia1513-1874.1983.09.175

 

USE OF 20% SE-30 ON CHROMOSORB P-AW-DMCS, 60/80 MESH,FOR SEP A-RATION OF n-ALKANES (C6 - C17), I-ALKENES (C5 - C10), AROMATICS (BENZENE AND MONOSUBSTITUTED n-ALKYL (C1 - C10) BENZENES)

 

PROESPICHAYA KANATHARANAa and R.L. GROBb

ABSTRACT: The 20% SE-30 on Chromosorb P-A W-DMCS, 60/80 mesh as a column packing in six feet,. 1/4" D.D. glass column at the optimum conditions, i.e., temperature programmed between 60 oC - 300 oC, detector temperature 310 oC, injection port temperature 320 oC, helium carrier gas flow rate 65 ml/minute, flow ratio of H2 : He : Air, 1 : 2 : 7 and dual flame ionization detector gave baseline separation of n-alkanes (C6 - C17), I-alkenes (C5 - C10) and aromatics (benzene and monosubstituted n-alkyl (C1 - C10) benzene). The separation of the hydrocarbon mixture of n-alkanes (C6 - C17), I-alkenes (C5 - C10) and aromatics (benzene and monosubstituted n-alkyl (C1 - C10) benzene) also can be achieved from this column.

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a. Department of Chemistry, Faculty of Science, Prince of Songkla University, Hat Yai, Thailand
b. Department of Chemistry, Villanova University, Villanova, Pa. 19085, U.S.A.

Received 26 November 1982